Chem 454 -review notes
Final Exam will focus, about 50-60% on materials since the last hour exam
Chapter 22 Electroanalytical methods
Chapter 23
Potentiometry
Chapter 24 Coulometry (only basic concept, Faraday's Law)
Chapter 25
Voltammetry
Chapter 26 Chromatography
- calculate N, H, internal standards
Chapter 27 GC
Chapter 28 HPLC
Chapter 29- Supercritical Fluids-- not included
Chapter 30- Capillary Electrophoresis
(only basic concept)
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Some of the Material Previously Covered
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bold = focus here; high danger of appearing on final
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tiny italics = not included on final
regular type = limited attention on final
Chapter 1-- Introduction
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end of chapter covers standardization methods
Chapter 2- Electrical Components
- except electronics as needed in later chapters
Chapter 3- Instrumentation Amplifiers
Chapter 4- Digital Electronics and Computers
except as needed in later chapters
Chapter 5- Signals and Noise
- should include statistics
- signal conditioning methods (cleaning up)
- frequencies
Chapter 6- Spectroscopic Methods
Chapter 7-- Optical Components
check out total internal reflection, fiber optics
grating, detectors, light sources, optical materials
will not include lasers
Chapter 8- Atomic Spectroscopy
- just the ideas critical to chapter 9
Chapter 9- AA and Atomic Fluorescence
Chapter 10 - AES
Chapter 11 Atomic Mass Spectrometry
Chapter 12 Atomic X-Ray Spectra
Chapter 13 Molecular UV-Vis Spectra
Chapter 14 - Applications of Absorption Spectra
- certainly should be able to do Beer's Law including
- mixtures; absorbances and %T
Chapter 15- Fluorescence / Luminescence
Chapter 16- Intro to IR
includes Fourier Transform Instruments
Chapter 17- Applications of IR
- include ATR method , cells and windows
Chapter 18- Raman Spectra
Chapter 19- NMR and ESR
Chapter 20- Mass Spectra
Chapter 21- Surface Characterization
Chapter 31 Thermal Methods
Chapter 32 Radiochemical Methods
Chapter 33 Automated Methods of Analysis
Important Question type:
1. What would be a good instrument technique if you were asked to determine xxxxxxxxxxx ?
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why?
- what are the alternatives?
- and important limits?
2. Would the instrument xxxxxxxxxx be useful if you were asked to determine yyyyyyy? (why?)